Volume 39 Issue 5
Sep.  2019
Turn off MathJax
Article Contents
Article Navigation >  Journal of Aeronautical Materials  > 2019  >  39(5): 13-23
Xiaoxu LYU, Zhe QI, Wenqing ZHAO, Zhuyu JIANG, Jinhua YANG, Yiran ZHOU, Hu LIU, Jian JIAO. Research progress of BN interphase and its multilayers in SiCf/SiC composites[J]. Journal of Aeronautical Materials, 2019, 39(5): 13-23. doi: 10.11868/j.issn.1005-5053.2019.000101
Citation: Xiaoxu LYU, Zhe QI, Wenqing ZHAO, Zhuyu JIANG, Jinhua YANG, Yiran ZHOU, Hu LIU, Jian JIAO. Research progress of BN interphase and its multilayers in SiCf/SiC composites[J]. Journal of Aeronautical Materials, 2019, 39(5): 13-23. 10.11868/j.issn.1005-5053.2019.000101
shu

Research progress of BN interphase and its multilayers in SiCf/SiC composites

doi: 10.11868/j.issn.1005-5053.2019.000101
  • 1.

    National Key Laboratory of Advanced Composites, AECC Beijing Institute of Aeronautical Materials, Beijing 100095, China

  • 2.

    School of Materials Science & Engineering, Beijing Institute of Technology, Beijing 100081, China

  • Received Date: 2019-06-10
  • Rev Recd Date: 2019-07-23
    • Available Online: 2019-09-06
  • Publish Date: 2019-09-27
    Abstract
  • SiCf/SiC composites are consisted of SiC fibers, SiC matrix and interphase. The interphase can transfer stresses from matrix to SiC fibers and deflects microcracks, at the same time, it protects SiC fibers from chemical erosion during the preparation and use of materials, which plays a very important role in regulating the properties of SiCf/SiC composites. In this paper, the effects of precursor gas ratio, carrier gas, deposition pressure, temperature on the deposition rate and microstructure of interphase during the chemical vapor infiltration (CVI) process are summarized. It will be the key and difficult point in the research of SiCf/SiC composite interphase to select appropriate process conditions and prepare BN and its composite multilayer with ideal structure.

     

    • FullText(HTML)
  • loading
    • References(67)
  • [1] NASLAIN R. Design,preparation and properties of non-oxide CMCs for application in engines and nuclear reactors: an overview[J]. Composites Science & Technology,2004,64(2):155-170.
    [2] NASIRI N A,PATRA N,NI N,et al. Oxidation behaviour of SiC/SiC ceramic matrix composites in air[J]. Journal of the European Ceramic Society,2016,36(14):3293-3302. doi: 10.1016/j.jeurceramsoc.2016.05.051
    [3] 刘虎,杨金华,周怡然,等. 国外航空发动机用SiCf/SiC复合材料的材料级性能测试研究进展[J]. 材料工程,2018,46(11):1-12. doi: 10.11868/j.issn.1001-4381.2018.000503

    LIU H,YANG J H,ZHOU Y R,et al. Progress in coupon tests of SiCf/SiC ceramic matrix composites used for aero engines[J]. Journal of materials engineering,2018,46(11):1-12.) doi: 10.11868/j.issn.1001-4381.2018.000503
    [4] STAEHLER J M,ZAWADA L P. Performance of four ceramic-matrix composite divergent flap inserts following ground testing on an F110 turbofan engine[J]. Journal of the American Ceramic Society,2010,83(7):1727-1738.
    [5] 周怡然,刘虎,杨金华,等. 熔融渗透工艺制备SiC-TiSi2复相陶瓷的反应机理[J]. 材料工程,2019,47(6):88-93. doi: 10.11868/j.issn.1001-4381.2018.001449

    ZHOU Y R,LIU H,YANG J H,et al. Reaction mechanism of SiC-TiSi2 by melt infiltration method[J]. Journal of Materials Engineering,2019,47(6):88-93.) doi: 10.11868/j.issn.1001-4381.2018.001449
    [6] CHARLES H,HENAGER J,KURTZ R J. Low-activation joining of SiC/SiC composites for fusion applications[J]. Journal of Nuclear Materials,2011,417(1/2/3):375-378. doi: 10.1016/j.jnucmat.2010.12.084
    [7] HINO T,HAYASHISHITA E,YAMAUCHI Y,et al. Helium gas permeability of SiC/SiC composite used for in-vessel components of nuclear fusion reactor[J]. Fusion Engineering and Design,2005,73(1):51-56. doi: 10.1016/j.fusengdes.2005.01.002
    [8] SPITSBERG I,STEIBEL J. Thermal and environmental barrier coatings for SiC/SiC CMCs in aircraft engine applications[J]. Applied Ceramic Technology,2010,1(1):291-301.
    [9] 杨金华,吕晓旭,焦健. 碳化硅陶瓷基复合材料界面层技术研究进展[J]. 航空制造技术,2008,61(11):79-87. doi: 10.3969/j.issn.1671-833X.2008.11.016

    YANG J H,LV X X,JIAO J. Progress in interphase technology of silicon carbide matrix composites[J]. Aeronautical Manufacturing Technology,2008,61(11):79-87.) doi: 10.3969/j.issn.1671-833X.2008.11.016
    [10] SHANTI V N, KARL J. High temperature mechanical behavior of ceramic composites[M]. Massachusetts, Butterworth-Heinemann, 1995: 6-7.
    [11] NASLAIN R R. The design of the fibre-matrix interfacial zone in ceramic matrix composites[J]. Composites:Part A,1998,29(9/10):1145.
    [12] SREEJITH K,VIPIN V,SUBRAMANIA S,et al. A comparative study on Cf/PyC/SiC minicomposites prepared via CVI process for hypersonic engine application[J]. International Journal of Applied Ceramic Technology,2018,15(5):1110-1123. doi: 10.1111/ijac.12898
    [13] WINDISCH C F,HENAGER C,SPRINGER G D,et a1. Oxidation of the carbon interface in Nicalon fiber reinforced silicon carbide composite[J]. Journal of the American Ceramic Society,1997,80(3):569-574. doi: 10.1111/j.1151-2916.1997.tb02868.x
    [14] OPILA E J,VERRILLI M J. Borosilicate glass-induced fiber degradation of SiC/BN/SiC composites exposed in combustion environments[J]. International Journal of Applied Ceramic Technology,2016,13(3):434-442. doi: 10.1111/ijac.12499
    [15] NASLAIN R R,PAILLER R J F,LAMON J L. Single and multilayered interphases in SiC/SiC composites exposed to severe environmental conditions:an overview[J]. International Journal of Applied Ceramic Technology,2010,7(3):263-275.
    [16] WING B L,HALLORAN J W. Subsurface oxidation of boron nitride coatings on silicon carbide fibers in SiC/SiC ceramic matrix composites[J]. Ceramics International,2018,44(14):17499-17505. doi: 10.1016/j.ceramint.2018.06.221
    [17] 李琳琳,李爱军,彭雨晴,等. 化学气相沉积法制备氮化硼界面涂层的研究进展[J]. 宇航材料工艺,2016,46(4):8-12. doi: 10.3969/j.issn.1007-2330.2016.04.002

    LI L L,LI A J,PENG Y Q,et al. Progress on boron nitride interface coating achieved by CVD[J]. Aerospace Materials Technology,2016,46(4):8-12.) doi: 10.3969/j.issn.1007-2330.2016.04.002
    [18] OPILA E,BOYD M K. Oxidation of SiC fiber-reinforced SiC matrix composites with a BN interphase[J]. Materials Science Forum,2010,696:342-347.
    [19] MU Y,ZHOU W C,WANG C,et al. Mechanical and electromagnetic shielding properties of SiCf/SiC composites fabricated by combined CVI and PIP process[J]. Ceramics International,2014,40(7):10037-10041. doi: 10.1016/j.ceramint.2014.02.103
    [20] PARK J Y,KIM D J,KIM W J. Characterization of SiC ceramic tube prepared by the combined CVI and CVD process[J]. Advances in Science & Technology,2014,94:38-42.
    [21] TAY R Y,LI H,TSANG S H,et al. Trimethylamine borane: a new single-source precursor for monolayer h-BN single crystals and h-BCN thin films[J]. Chemistry of Materials,2016,28(7):2180-2190. doi: 10.1021/acs.chemmater.6b00114
    [22] REBILLAT F,GUETTE A,BROSSE C R. Chemical and mechanical alterations of SiC Nicalon fiber properties during the CVD/CVI process for boron nitride[J]. Acta Materialia,1999,47(5):1685-1696. doi: 10.1016/S1359-6454(99)00032-4
    [23] JACQUES S,VINCENT H,VINCENT C,et al. Multilayered BN coatings processed by a continuous LPCVI treatment onto Hi-Nicalon fibers[J]. Journal of Solid State Chemistry,2001,162(2):358-363. doi: 10.1006/jssc.2001.9387
    [24] HANNACHE H,QUENISSET J M,NASLAIN R,et al. Composite materials made from a porous 2D-carbon-carbon preform densified with boron nitride by chemical vapour infiltration[J]. Journal of Materials Science,1984,19(1):202-212. doi: 10.1007/BF02403127
    [25] JACQUES S,LOPEZ M A,VINCENT C,et a1. Bouix SiC/SiC minicomposites with structure-graded BN interphases[J]. Journal of the European Ceramic Society,2000,20(12):1929-1938. doi: 10.1016/S0955-2219(00)00064-9
    [26] DUGNE O,PROUHET S,GUETTE A,et al. On a thermodynamic approach to the chemical phenomena involved in the formation of a BN interphase by CVD/CVI from a BF3-NH3 precursor[J]. Journal of Alloys and Compounds,1992,176(2):187-213.
    [27] PROUHET S,LANGLAIS F,GUETTE A,et al. On the kinetics of boron nitride CVD from BF3-NH3-Ar. Part 2:influence of the precursor composition and chemical mechanisms[J]. Chem Inform,1994,25(10).
    [28] CARMINATI P,BUFFETEAU T,DAUGEY N,et a1. Low pressure chemical vapour deposition of BN: relationship between gas phase chemistry and coating microstructure[J]. Thin Solid Films,2018,664:106-114. doi: 10.1016/j.tsf.2018.08.020
    [29] CHOLET V,VANDENBULCKE L. Chemical vapor infiltration of boron nitride interphase in ceramic fiber preforms: discussion of some aspects of the fundamentals of the isothermal chemical vapor infiltration process[J]. Journal of the American Ceramic Society,2010,76(11):2846-2858.
    [30] HUANG J,PAN C,LI D. Investigation of the BN films prepared by low pressure chemical vapor deposition[J]. Surface & Coatings Technology,1999,122(2/3):166-175.
    [31] EDWARD K N,STEVEN L S. Experimental design in the deposition of BN interface coatings on SiC fibers by chemical vapor deposition[J]. Surface & Coatings Technology,2006,201(6):2741-2748.
    [32] CHOI B J. Chemical vapour deposition of hexagonal boron nitride films[J]. Materials Research Bulletin,1999,34(14/15):2215-2220.
    [33] MOTOJIMA S,TAMURA Y,SUGIYAMA K. Low temperature deposition of hexagonal BN films by chemical vapour deposition[J]. Thin Solid Films,1982,88(3):269-274. doi: 10.1016/0040-6090(82)90056-6
    [34] LEE W Y,LACKEY W J,AGRAWAL P K. Kinetic analysis of chemical vapor deposition of boron nitride[J]. Journal of the American Ceramic Society,1991,74(10):2642-2648. doi: 10.1111/j.1151-2916.1991.tb06813.x
    [35] MICHIYUKI S,YOSHIZUMI T,YOSHIYUKI I,et a1. Properties of BN coating on SiC fiber by continuous CVD process[J]. The Journal of American Ceramic Society,2006:144.
    [36] PATIBANDLA N. Chemical vapor deposition of boron nitride[J]. Journal of the Electrochemical Society,1992,139(12):3558-3565. doi: 10.1149/1.2069121
    [37] 王梦千,贾林涛,李爱军,等. BCl3-NH3-H2-N2前驱体化学气相沉积法制备氮化硼涂层[J]. 无机材料学报,2018,33(11):1179-1185.

    WANG M Q,JIA L T,LI A J,et al. Preparation of boron nitride coating from BCl3-NH3-H2-N2 precursor by chemical vapor deposition[J]. Journal of Inorganic Materials,2018,33(11):1179-1185.)
    [38] PEDERSEN H,CHUBAROV M,HGBERG H,et a1. On the effect of water and oxygen in chemical vapor deposition of boron nitride[J]. Thin Solid Films,2012,520(18):5889-5893. doi: 10.1016/j.tsf.2012.05.004
    [39] MENG C X,LI Y F,WU H,et al. Structural transformation of h-BN overlayers on Pt (111) in oxidative atmospheres[J]. Physical Chemistry Chemical Physics,2018,20(16):11013-11020. doi: 10.1039/C8CP00877A
    [40] TAKASHI T,KOJI K,MASATAKA T,et al. Phase transformation of amorphous boron nitride under high pressure[J]. Chemistry of Materials,2003,15(14):2744-2751. doi: 10.1021/cm021763j
    [41] GALLET S L,CHOLLON G,REBILLAT F,et a1. Microstructural and microtextural investigations of boron nitride deposited from BCl3-NH3-H2 gas mixtures[J]. Journal of the European Ceramic Society,2004,24(1):33-44. doi: 10.1016/S0955-2219(03)00126-2
    [42] CHENG Y,YIN X W,LIU Y S,et al. BN coatings prepared by low pressure chemical vapor deposition using boron trichloride-ammonia-hydrogen-argon mixture gases[J]. Surface & Coatings Technology,2010,204(16/17):2797-2802.
    [43] YANG M,ZHOU W C,LUO F,et al. Effects of BN/SiC dual-layer interphase on mechanical and dielectric properties of SiCf/SiC composites[J]. Ceramic International,2014(40):3411-3418.
    [44] BERTRAND S,BOISRON O,PAILLER R,et al. (PyC-SiC)n and (BN-SiC)n nano-scale multilayered interphases by pressure pulsed-CVI[J]. Key Engineering Materials,1999,164/165:357-360.
    [45] LI J P,QIN H L,LIU Y S,et al. Effect of the SiCl4 Flow Rate on SiBN deposition kinetics in SiCl4-BCl3-NH3-H2-Ar environment[J]. Materials,2017,10(6):627. doi: 10.3390/ma10060627
    [46] LIU Y S,CHAI N,LI Z,et al. Effect of deposition temperature on deposition kinetics and mechanism of silicon boron nitride coating deposited from SiCl4-BCl3-NH3-H2-Ar mixture using low pressure chemical vapor deposition[J]. Surface & Coatings Technology,2015,261(3):295-303.
    [47] UDAYAKUMAR A,GANESH S,RAJA M. Effect of intermediate heat treatment on mechanical properties of SiCf/SiC composites with BN interphase prepared by ICVI[J]. Journal of the European Ceramic Society,2011,31(6):1145-1153. doi: 10.1016/j.jeurceramsoc.2010.12.018
    [48] NASLAIN R. The concept of layered interphases in SiC/SiC[J]. Ceramic Transactions,1995,58:23-39.
    [49] YANG B,ZHOU X G,CHAI Y X. Mechanical properties of SiCf/SiC composites with PyC and the BN interface[J]. Ceramics International,2015,41(5):7185-7190. doi: 10.1016/j.ceramint.2015.02.041
    [50] WANG L J,CHEN Z K,WANG B W,et al. Effect of free carbon on micro-mechanical properties of a chemically vapor deposited SiC coating[J]. Ceramics International,2018,44(14):17118-17123. doi: 10.1016/j.ceramint.2018.06.165
    [51] ZHANG W G,HUTTINGER K J. CVD of SiC from methyltrichlorosilane. Part I: deposition rates[J]. Chemical Vapor Deposition,2001,7(4):167-172. doi: 10.1002/1521-3862(200107)7:4<167::AID-CVDE167>3.0.CO;2-L
    [52] HUO Y L,CHEN Y F. Effect of gas flow and gas ratio on CVD SiC coating[J]. Journal of Synthetic Crystal,2009,38:255-258.
    [53] MENG F T,DU S Y,ZHANG Y M. Characterization of silicon carbide films prepared by chemical vapor deposition[J]. Advanced Materia & Research,2011,177:78-81.
    [54] 刘荣军,张长瑞,刘晓阳,等. CVI过程中温度对SiC 涂层沉积速率及组织结构的影响[J]. 航空材料学报,2004,24(4):22-26. doi: 10.3969/j.issn.1005-5053.2004.04.006

    LIU R J,ZHANG C R,LIU X Y,et al. The effects of deposition temperature on the deposition rates and structures of CVD SiC coatings[J]. Journal of Aeronautical Materials,2004,24(4):22-26.) doi: 10.3969/j.issn.1005-5053.2004.04.006
    [55] LONG Y,JAVED A,CHEN Z. Deposition rate, texture, and mechanical properties of SiC coatings produced by chemical vapor deposition at different temperatures[J]. International Journal of Applied Ceramic Technology,2013,10(1):11-19. doi: 10.1111/j.1744-7402.2012.02786.x
    [56] XU Y,CHENG L,ZHANG L,et a1. Morphology and growth mechanism of silicon carbide chemical vapor deposited at low temperatures and normal atmosphere[J]. Journal of Materials Science,1999,34(3):551-555. doi: 10.1023/A:1004546712932
    [57] BENAMI A,SANTANA G,ORTIZ A,et al. Strong white and blue photoluminescence from silicon nanocrystals in SiNx grown by remote PECVD using SiCl4/NH3[J]. Nanotechnology,2007,18(15):155704-155708. doi: 10.1088/0957-4484/18/15/155704
    [58] 尹立峰,王思青,张长瑞,等. 制备工艺对CVD Si3N4涂层沉积速率的影响[J]. 材料导报,2008,22(5):415-417.

    YIN L F, WANG S Q,ZHANG C R,et al. Effects of preparation technique on deposition rate of silicon nitride by low pressure chemical vapor deposition[J]. Materials Review,2008,22(5):415-417.)
    [59] KWATERA A,SAWKA A,KWATERA D. Amorphous Si3N4 layers synthesized on cemented carbide tools using an atmospheric pressure CVD method[J]. Surface & Coatings Technology,1997,88(1):12-16.
    [60] CHAI Y X,ZHANG H Y,ZHOU X G. Mechanical properties of SiCf/SiC composites with alternating PyC/BN multilayer interfaces[J]. Advances in Applied Ceramics,2017,116(7):392-399. doi: 10.1080/17436753.2017.1339517
    [61] 张伟刚. 化学气相沉积[M]. 北京: 科学出版社. 2007.

    ZHANG W G. Chemical vapor deposition[M].Beijing: Science Press, 2007.
    [62] NORINAGA K,JANARDHANAN V M,DEUTSCHMANN O. Detailed chemical kinetic modeling of pyrolysis of ethylene, acetylene, and propylene at 1073-1373 K with a plug-flow reactor model[J]. International Journal of Chemical Kinetics,2008,40(4):199-208. doi: 10.1002/kin.20302
    [63] PAUW D V,KALHOFER S,GERTHSEN D. Influence of the deposition parameters on the texture of pyrolytic carbon layers deposited on lanar substrates[J]. Carbon,2004,42(2):279-286. doi: 10.1016/j.carbon.2003.10.027
    [64] HU Z J,ZHANG W G,HÜTTINGER K J,et al. Influence of pressure, temperature and surface area/volume ratio on the texture of pyrolytic carbon deposited from methane[J]. Carbon,2003,41(4):749-758. doi: 10.1016/S0008-6223(02)00403-7
    [65] ISABELLE Z,RENE F,PAUL M M. Pyrolysis of propane for CVI of pyrocarbon part Ⅲ:experimental and modeling study of the formation of pyrocarbon[J]. Journal of Analytical and Applied Pyrolysis,2007,79(1):268-277.
    [66] 赵春年,成来飞,张立同,等. 丙烯化学气相沉积热解碳的动力学研究[J]. 无机材料学报,2008,23(6):1165-1170. doi: 10.3321/j.issn:1000-324X.2008.06.016

    ZHAO C N,CHENG L F,ZHANG L T,et al. Kinetics study in chemical vapor deposition of pyrocarbon from pyropylene[J]. Journal of Inorganic Materials,2008,23(6):1165-1170.) doi: 10.3321/j.issn:1000-324X.2008.06.016
    [67] LACROIX R,FOURNET R,ZIEGLER D I. Kinetic modeling of surface reactions involved in CVI of pyrocarbon obtained by propane pyrolysis[J]. Carbon,2010,48(1):132-144. doi: 10.1016/j.carbon.2009.08.041
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(8)  / Tables(2)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views (4864) PDF downloads(101) Cited by()
    Proportional views
    Related

    Copyright © 2015 Editorial Board of Journal of Aeronautical Materials

    京ICP备15058934号-1

    Address：P.Q.BOX 81-44,Beijing 100095,China

     E-mail：info@hkclxb.cn

    Supported by Beijing Renhe Information Technology Co. Ltd   百度统计

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return